Conformation of the oleate chains in crystals of cholesteryl oleate at 123 K.

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Conformation of the oleate chains in crystals of cholesteryl oleate at 123 K.

At 123 K, crystals of cholesteryl cis-9-octadecenoate (cholesteryl oleate, C45H78O2) are monoclinic, space group P2(1) with unit cell dimensions a = 12.356(2), b = 8.980(3), c = 18.382(2) A, beta = 85.49(2) degrees, and have two molecules in the unit cell. The crystal structure including all H atoms has been determined from 3812 independent X-ray reflections with sin theta/lambda less than 0.61...

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Conformation and packing of unsaturated chains in cholesteryl linolelaidate at 123 K.

At 123 K, crystals of cholesteryl trans-9-trans-12-octadecadienoate (cholesteryl linolelaidate, C47H76O2) are monoclinic, space group P2(1) with cell dimensions a = 13.03(3), b = 8.76(2), c = 17.90(4) A, beta = 89.7(2) degrees, having two molecules per unit cell. The crystal structure has been determined from 2041 X-ray intensities with sin theta/lambda less than 0.48 A-1, of which 922 gave I g...

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Conformation and packing of unsaturated chains in cholesteryl linolelaidate at 123 K 1

At 123 K, crystals of cholesteryl trans-9-trans-1 2octadecadienoate (cholesteryl linolelaidate, C4,H,602) are monoclinic, space group P21 with cell dimensionsa = 13.03(3), b = 8.76(2), c = 17.90(4) A, @ = 89.7(2)", having two molecules per unit cell. T h e crystal structure has been determined from 2041 X-ray intensities with sin O/A < 0.48 A-', of which 922 gave I > 2cr(I). T h e hydrogen atom...

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A comparison of cholesteryl oleate and 19-iodocholesteryl oleate as substrates for adrenal cholesterol esterase.

Radiolabeled 19-iodocholesterol is widely used to obtain images of human adrenals. We have shown in rats and mice that 85-95% of the radiolabel is present in the esterified form. Using rat adrenal cytosolic cholesterol esterase, the kinetic parameters K~t and V were determined for commercially available cholesteryl [l-14C]-oleate (!) and [125I]-19-iodocholesteryl oleate (It). The Kra and V were...

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Solubilization of triolein and cholesteryl oleate in egg phosphatidylcholine vesicles.

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ژورنال

عنوان ژورنال: Journal of Lipid Research

سال: 1990

ISSN: 0022-2275

DOI: 10.1016/s0022-2275(20)38757-5